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By David Allen Shirley

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Bhupathy,and T. Cohen, Tetrahedron Letters,2E'2203(1987)' N,N'-Bis(salicylidene)ethylenediaminonickel(II), Ni(salen) (1). Supplier: Aldrich. ' Ni(salen). Styrenes oxidationof somealkeneswith NaOCI under phase-transfer Bis(himethylsilyl) setenide ttr'. r. are convertedmainly to epoxidesbut purely ariphaticalkenesare convertedto a mixture of products. ' H. YoonandC. J. Burrows, Am. ,ilO, 40g7(l9gg). )2 Bis(trimethylsilyl)setenide,[(CH3)rSi]rSe (t). )3siosi(cHJJ. )3SiSeLi,which can be regeneratedby a peterson-type elimination (equationI).

Coreyand D. Seebach, J. ,31' 4097(1966). : W. D. Abraham,M. Bhupathy,and T. Cohen, Tetrahedron Letters,2E'2203(1987)' N,N'-Bis(salicylidene)ethylenediaminonickel(II), Ni(salen) (1). Supplier: Aldrich. ' Ni(salen). Styrenes oxidationof somealkeneswith NaOCI under phase-transfer Bis(himethylsilyl) setenide ttr'. r. are convertedmainly to epoxidesbut purely ariphaticalkenesare convertedto a mixture of products. ' H. YoonandC. J. Burrows, Am. ,ilO, 40g7(l9gg). )2 Bis(trimethylsilyl)setenide,[(CH3)rSi]rSe (t).

Weigold, J. Organometal. 0). r Y. Ishii,T. Nakano, A. Inada,Y. Kishigami, K. Sakurai, andM. Ogawa,J. ,Sl,240 (1986); T. Nakano, Y. Ishii,andM. Ogawa, (1987). " of eolauu;, and of 3 to 4 involves Conversion yield' mixture of (E)- and (Z)-isomers in 66Vo a 2-silylfuranto a of oxidation oxygen reduction(DIBAH) and selectivesinglet butenolide. -azolr,S i(CH3)3 + \// HOHrC/- , r,""",,. uoo"ro,oou,, f I l19l (1987)' Leuers'2iE' rS. Katsumura, andS' Isoe'Tetrahedron S. Fuliwara, (BINAP)' Supplier: (R)- and (S)'2,2"Bis(diphenylphosphino)'1,1'-binaphthyl Fluka.

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Preparation of Organic Intermediates by David Allen Shirley


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